Low voltage BSE imaging using FESEM

نویسندگان

  • R. G. Richards
  • G. Rh. Owen
  • I. ap Gwynn
چکیده

Backscattered electron (BSE) imaging is most commonly performed by applying accelerating voltages of 10kV and above to the specimen. For imaging of surface detail, the application of a lower accelerating voltage results in less beam penetration, spread and overall specimen damage. A field emission scanning electron microscope (FESEM) operated with high emission current (50μA) was used to increase the number of BSE obtainable from imaged specimens. When operated with a high condenser lens current and a lower accelerating voltage (<5kV) the interaction volume of the electron beam with the specimen was minimised. The lower voltage BSE images exhibited enhanced surface detail and contrast. Specimens that normally charged, locally affecting secondary electron (SE) detection, were imaged without such distortions when BSE were used. It was advantageous to use a range of applied accelerating voltages in order to provide the most image information.

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

منابع مشابه

High Resolution Backscatter Electron ( Bse ) Imaging of Immunogold with in - Lens and below - the - Lens Field Emission Scanning Electron Microscopes

High resolution backscatter electron (BSE) imaging of colloidal gold with field emission scanning electron microscopy (FESEM) depends upon selection of accelerating voltage, beam current, working distance between specimen and backscatter detector, type of backscatter detector, plus the nature and thickness of the metal coating used to improve conductivity and signal collection. BSE imaging of a...

متن کامل

Backscattered electron (BSE) imaging of platinum nano-particles dispersed in mesoporous silica.

High-resolution scanning electron microscopy (HR-SEM) with backscattered electrons (BSE) under a low accelerating voltage provided images with compositional information about Pt nano-particles with a diameter of approximately 6 nm that were dispersed in mesoporous silica (SBA-15). The dispersion of Pt nano-particles in mesoporous silica was investigated using the BSE imaging method in combinati...

متن کامل

n-ZnO nanorods/p+-Si (111) heterojunction light emitting diodes

In this study, we report the effects of thermal annealing in nitrogen ambient on the optical and electrical properties of zinc oxide (ZnO) nanorod (NR) arrays for the application in light emission diodes (LED). The single-crystalline ZnO NR array was synthesized on p+-Si (111) substrate without seed layer using simple, low-cost, and low-temperature hydrothermal method. The substrate surface was...

متن کامل

Influence of topography and specimen preparation on backscattered electron images of bone.

Backscattered electron (BSE) images of bone exhibit graylevel contrast between adjacent lamellae. Mathematical models suggest that interlamellar contrast in BSE images is an artifact due to topographic irregularities. However, little experimental evidence has been published to support these models, and it is not clear whether submicron topographical features will alter BSE graylevels. The goal ...

متن کامل

Employing dual frequency phase sensitive demodulation technique to improve the accuracy of voltage measurement in magnetic induction tomography and designing a labratoary prototype

Magnetic induction tomography (MIT) is a promising modality for noninvasive imaging due to its contactless technology. Being a non-contact safe imaging technique, MIT has been an appropriate method in compare to other electrical tomography. In this imaging method, a primary magnetic field is applied by excitation coils to induce eddy currents in the material to be studied and a secondary magnet...

متن کامل

ذخیره در منابع من


  با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

عنوان ژورنال:

دوره   شماره 

صفحات  -

تاریخ انتشار 2002